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Intermediates

N-(3-Acetyl-4-Hydroxy Phenyl) N, N-Diethyl Urea

 

 
Synonyms N, N-Diethyl Urea N-(3-Acetyl-4-Hydroxy Phenyl)
Molecular Formula

C13H18N2O3

Molecular Weight 250.13
CAS Number 79881-89-3

 
S. No. Test Specification
1 Description

A pale yellow to light brown crystalline powder

2 Solubility

Soluble in acetone,chloroform,benzene and insoluble in water

3 Identification by IR IR spectrum of sample should be similar to in-house standard.
4 Loss on drying
Not more than 1.0%
5 Melting range in degree centrigrade 140 - 142
6 Sulphated ash Not more than 0.2%
7 Related impurities by HPLC  
a) Individual impurity Not more than 1.0%
b) Total impurity Not more than 1.5%
8 Purity by HPLC Not less than 98.5%
9 End use Intermediate for Celiprolol

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