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Intermediates

4-Methoxy-3, 5-Dimethyl-2-Chloro Methyl Pyridine Hydrochloride (Chloro Compound)

 

 
Synonyms 4-Methoxy-3,5-dimethyl pyridine-2-chloro Methyl Hydrochloride
Molecular Formula

C9H13NOCl2

Molecular Weight 222.10
CAS Number 86604-75-3

 
S. No. Test Specification
1 Description A white to creamish white colour crystalline powder
2 Solubility

Freely soluble in methanol, methylene chloride, water, insoluble in acetone and toluene

3 Identification by IR The Infrared absorption spectrum of sample should be similar to in-house standard
4 Melting range in degree centrigrade 125 - 132
5 Loss on drying Not more than 1.0%
6 Purity by HPLC Not less than 98.0%
7 Residual solvents
by GC
 
a) Acetone Not more than 5000 ppm
b) Methanol Not more than 3000 ppm
c) Dichloro methane Not more than 600 ppm
d) Toluene Not more than 890 ppm
8 End use Intermediate for Omeprazole

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